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Free Books / Science / Distillation Principles And Processes / | ![]() |
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Carrying Out A Fractional Distillation. Part 5 |
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This section is from the book "Distillation Principles And Processes", by Sydney Young. Also available from Amazon: Distillation Principles And Processes.
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I. |
II. |
III. |
IV. |
V. |
VI. |
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F. |
t. |
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F. |
t. |
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F. |
t. |
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F. |
t. |
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F. |
t. |
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F. |
t. |
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A |
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1 |
(57.7°) |
1 |
57.3° |
63 |
31 5 |
||||||||||||||||||
|
2 |
(58.4°) |
2 |
58.6 |
17.2 |
191 |
2 |
58.2o |
19.4 |
176 |
2 |
58.2 |
28.5 |
31 7 |
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|
3 |
(60.9°) |
3 |
60.95 |
36.5 |
14.3 |
3 |
610 |
58.1 |
23.7 |
3 |
60.7 |
69.9 |
280 |
3 |
60.1 |
550 |
29.0 |
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|
4 |
(63.8°) |
4 |
63.8 |
59.7 |
20 6 |
4 |
63.85 |
77.2 |
26 6 |
4 |
63.9 |
53.1 |
183 |
4 |
63.85 |
49.0 |
153 |
4 |
63.85 |
54.2 |
143 |
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|
5 |
71.3 |
141.4 |
189 |
5 |
71.0 |
134.2 |
18.6 |
5 |
71.0 |
100.6 |
140 |
5 |
71.05 |
85.1 |
118 |
5 |
71.0 |
69.0 |
96 |
5 |
70.75 |
47.4 |
6.9 |
|
6 |
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7 |
7 |
7 |
75.7 |
52.-0 |
10.4 |
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|
8 |
77.8 |
145.2 |
22 3 |
8 |
77.1 |
98.4 |
161 |
8 |
77.15 |
75.4 |
12.4 |
8 |
77.15 |
66.6 |
109 |
8 |
7715 |
71.1 |
116 |
8 |
77.15 |
33.4 |
22 3 |
|
9 |
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|
10 |
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|
11 |
89.2 |
146.9 |
12.8 |
11 |
84.4 |
67.2 |
9.2 |
11 |
84.4 |
67.7 |
93 |
11 |
84.3 |
84.7 |
118 |
11 |
83.35 |
85.1 |
136 |
11 |
78.4 |
34.8 |
29 0 |
|
l2 |
19 |
82.5 |
47.9 |
11.7 |
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|
13 |
13 |
91.7 |
51.0 |
70 |
13 |
91.65 |
59.6 |
82 |
13 |
91.6 |
40.8 |
5.6 |
13 |
90.75 |
33.7 |
4.6 |
13 |
90.2 |
28-1 |
3.6 |
|||
|
14 |
{ above} 89.2 |
143.3 |
14 |
98.4 |
86.1 |
127 |
14 |
98.4 |
46.7 |
69 |
14 |
98.4 |
33.8 |
50 |
14 |
98.45 |
33.5 |
4.4 |
14 |
98.45 |
27.8 |
33 |
|
|
15 |
15 |
101.-5 |
63.7 |
20 6 |
15 |
101.45 |
78.3 |
261 |
15 |
100.95 |
44.1 |
17.6 |
15 |
100.95 |
29.4 |
118 |
15 |
100.95 |
25.6 |
102 |
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|
16 |
16 |
101.45 |
38.7 |
77.4 |
16 |
101.45 |
36.7 |
73.4 |
16 |
101.45 |
30.3 |
606 |
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|
17 |
17 |
(101.55) |
14.3 |
. . |
17 |
101.55 |
19.7 |
1970 |
17 |
101.55 |
24.2 |
242 0 |
17 |
101.55 |
31.1 |
310 |
17 |
101.55 |
340 |
3400 |
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X |
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|
Y |
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Z |
Z |
• • |
100 |
|
Z |
• • |
20.2 |
|
Z |
• • |
34.7 |
|
Z |
• * |
50.6 |
|
|||||||
|
576.8 |
574.6 |
571.7 |
566.6 |
562.6 |
555.9 |
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VII. |
VIII. |
XII. |
XVI. |
XX. |
XXIV. |
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F. |
T. |
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F. |
t. |
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F. |
t. |
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F. |
t. |
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F. |
t. |
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F. |
t. |
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|
A |
57.1° |
6.0 |
|
A |
57.1° |
411 |
|
A |
57.1° |
79.9 |
|
A |
57.1° |
105.5 |
|
A |
105.5 |
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|
1 |
57.3° |
13.3 |
66.5 |
1 |
57.3 |
11.7 |
585 |
1 |
57.2 |
17.0 |
1700 |
1 |
57.2 |
14.6 |
1460 |
1 |
57.15 |
5.9 |
1180 |
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2 |
58.2 |
42.9 |
47.7 |
2 |
58.2 |
491 |
546 |
2 |
57.65 |
30.5 |
67.8 |
2 |
57.6 |
17.3 |
43 2 |
2 |
57.55 |
10.7 |
26.7 |
B &C |
21.7 |
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|
3 |
60.0 |
47.5 |
26.4 |
3 |
60.1 |
45.4 |
239 |
3 |
58.9 |
303 |
24.2 |
3 |
58.6 |
14.6 |
146 |
3 |
58.55 |
8.9 |
8.9 |
D |
10.0 |
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|
4 |
63.8 |
43.5 |
11.4 |
4 |
63.8 |
360 |
97 |
4 |
63.5 |
31.0 |
6.7 |
4 |
65.35 |
25.0 |
3.7 |
4 |
67.25 |
17.6 |
20 |
4 |
67.2° |
6.8 |
08 |
|
5 |
70.75 |
45.9 |
6.7 |
5 |
70.7 |
37.8 |
5.5 |
5 |
71.9 |
23.8 |
28 |
5 |
73.9 |
15.6 |
1.8 |
5 |
75.95 |
16.6 |
1.9 |
5 |
75.3 |
15.1 |
1.9 |
|
7 |
75.8 |
42.7 |
8.4 |
7 |
75.8 |
41.9 |
8.2 |
7 |
76.45 |
32.9 |
71 |
7 |
76.8 |
26.6 |
92 |
7 |
76.95 |
160 |
160 |
6 7 |
76.8 77.1 |
7.8 12.2 |
5.2 40.7 |
|
8 |
77.2 |
45.0 |
32 1 |
8 |
77.15 |
43.8 |
324 |
8 |
77.0 |
30.5 |
55 5 |
8 |
77.1 |
26.7 |
89 0 |
8 |
77.1.5 |
13.4 |
670 |
8 |
77.15 |
14.6 |
292.2 |
|
9 |
77.15 |
27.6 |
1840 |
9 |
77.15 |
390 |
7800 |
9 |
77.15 |
45.0 49.4 |
18880 |
9 |
77.15 |
31.9 26.9 |
very high |
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|
10 |
77.3 |
36.2 |
241 3 |
10 |
77.2 |
39.9 |
7980 |
10 |
77.2 |
10 |
77.15 |
||||||||||||
|
11 |
78.3 |
37.8 |
34.4 |
11 |
78.2 |
51.1 |
48.7 |
11 |
77.6 |
35.6 |
853 |
11 |
77.35 |
24.4 |
162 6 |
11 |
77.25 |
130 |
260 0 |
||||
|
12 |
82.1 |
41.1 |
108 |
12 |
81.1 |
341 |
11.8 |
12 |
78.85 |
18.7 |
149 |
12 |
77.9 |
11.6 |
21.1 |
||||||||
|
13 |
90.15 |
23.4 |
29 |
13 |
90 05 |
22.8 |
25 |
13 |
88.9 |
17.9 |
18 |
||||||||||||
|
14 |
98.45 |
22.3 |
27 |
14 |
98.5 |
17.8 |
21 |
14 |
99.55 |
9.5 |
09 |
||||||||||||
|
15 |
100.95 |
17.6 |
70 |
15 |
101.0 |
16.7 |
6.7 |
15 |
10115 |
8.1 |
51 |
||||||||||||
|
16 |
101.45 |
24.3 |
48.6 |
16 |
101.45 |
19.4 |
43.3 |
||||||||||||||||
|
17 |
101.55 |
23.7 |
2370 |
17 |
101.55 |
12.6 |
126 0 |
||||||||||||||||
|
X |
7.8 |
U |
6.6 |
S |
8.6 |
Q |
13-1 |
||||||||||||||||
|
Y |
81 |
||||||||||||||||||||||
|
Z |
• • |
80.2 |
|
Z |
101.5 |
|
Z |
« • |
132.6 |
|
172.4 |
TtoZ |
• • |
192.3 |
RtoZ |
228.8 |
|||||||
|
551.2 |
547.7 |
529.2 |
514.2 |
502.9 |
494.4 |
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Continue to:
liquids, distillation, vapour, boiling point, composition, still-head, mixtures, compositions, sublimation, alcohol, acetone, water, purification, pressure, tar, raw material, essential oils
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