This section is from "Scientific American Supplement". Also available from Amazon: Scientific American Reference Book.
Water that has been used to wash frozen beets contains a small percentage of sugar. As the washing period, in such cases, is longer than with normal beets, the sugar in beet cells has time to pass through the outer walls by osmosis. The sugar loss is said to be 0.66 per cent. (?) of the weight of beets washed.
Well conducted experiments show that in small but well ventilated silos, beets lose considerable weight, but very little sugar. On the other hand, in large silos with poor ventilation, the sugar loss frequently represents four to six per cent. When fermentation commences, the mass of roots is almost ruined.
Sodic nitrate, if used upon soil late in the season, may overcome a difficulty that has been recently noticed. Beet fields located near swamps that are dry a portion of the year have suffered from a malady that turns leaves from green to yellow, even before harvesting period; such beets have lost a considerable amount of sugar.
A new method for the analysis of saccharose and raffinose, when in the presence of inverted sugar, is said to give accurate results. The process consists in adding sulphate of copper and lime to hot molasses, so that the oxide of copper is changed to a protoxide, and the invert sugar becomes water and carbonic acid. The whole is neutralized with phosphoric acid. There follow a great number of precipitates; the exact volume of liquid in which these are found is determined after two polariscopic observations.
It has been constantly noticed that samples of carbonatated juice vary in composition with the part of tank from which they are taken. If some arrangement could be made assuring a thorough mixing during the passage of carbonic acid, results would be more satisfactory than they now are. If gas could be distributed in every part of the tank, the lime combination could be made perfect.
Notwithstanding the new law regulating quantity of sugar to be used in wines, ciders, etc., there has been, during 1890, an increase of nearly 13,000 tons, as compared with 1889. Consumption of sugar for these special industries was 33,000 tons; alcohol thus added to wine was about 71,000,000 gallons.
Beets cultivated without extra fertilizers, and that are regular in shape and in good condition, without bruises, are the ones which give the best results in silos. It is recommended to construct silos of two types; one which is to be opened before first frost, the other where beets remain for several months and are protected against excessive cold. Great care should be taken that a thorough ventilation be given in the first mentioned type. In the other, more substantial silos, ventilation must be watched,and all communication with the exterior closed as soon as the temperature falls to or near freezing.
During the last campaign many manufacturers experienced great difficulty in keeping the blades of slicers sufficiently sharp to work frozen beets. Sharpening of blades is an operation attended to by special hands at the factory; and under ordinary circumstances there need be no difficulty. However, it is now proposed to have central stations that will make a specialty of blade sharpening. Under these circumstances manufacturers located in certain districts need give the matter no further thought, let the coming winter be as severe as it may.
Some success has been obtained by the use of sulphurous acid in vacuum pans. Great care is required; the operation cannot be done by an ordinary workman. It is claimed that graining thereby is more rapid and better than is now possible. Chemists agree that the operation is more effectual by bringing sulphurous acid in contact with sirups rather than juices; it is in the sirups that the coloring pigments are found. Sulphurous acid is run into the pan until the sirups cover the second coil. In all cases the work must be done at a low temperature.
Height of juice in carbonatating tanks is only three feet in France, while in Austria it is frequently twelve feet. The question of a change in existing methods is being discussed; it necessitates an increase in the blowing capacity of machine; since carbonic acid gas has a greater resistance to overcome in Austrian than in French methods. Longer the period juices are in contact with carbonic acid, greater will be the effect produced.
Ferric sulphate has been very little used for refuse water purification, owing to cost of its manufacture. If roasted pyrites, a waste product of certain chemical factories, are sprinkled with sulphuric acid of 66° B., and thoroughly mixed for several hours, at a temperature of 100° to 156° F., the pyrites will soon be covered with a white substance which is ferric sulphate. Precipitates from ferric sulphate, unlike calcic compounds, do not subsequently enter into putrefaction.
Efforts are being made to convince manufacturers of the mistake in using decanting vats, in connection with first and second carbonatation. In Germany filter presses are used, decanting vats are obsolete. The main objection to them is cooling of saccharine liquors, which means an ultimate increase in fuel. Cooling is frequently followed by partial fermentation.
Further changes in the proposed combined baryta-soda method for juice purification consist in using powdered soda carbonate 90-92°, upon beet cossettes as they leave the slicer, before entering the diffusor. The quantity of chemical to be used is 1/1000 of weight of beet slices being treated. If a diffusor has a capacity of 2,500 lb., there would be added 2.5 lb. soda carbonate. From the diffusor is subsequently taken 316 gallons juice at 4-5° density, this is rapidly heated to 185°F., then 2.4 of a pure baryta solution is added; temperature is kept at 185° F. for a short time; resulting precipitates fall to bottom of tank; then 13 gallons milk of lime 25° B. are added.
Other operations that follow are as usual. It is contended that the cost of baryta is 10 cents per ton beets worked. The most important advantage is gain in time; a factory working 20,000 during a 100-day campaign, by the foregoing process can accomplish the same work in 80 days, thus decreasing wear and tear of plant and diminishing percentage of sugar lost in badly constructed silos.
 
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