This section is from the "Henley's Twentieth Century Formulas Recipes Processes" encyclopedia, by Norman W. Henley and others.
Take of a mixture made of:
2/3 Sapan wood..............56 parts
1/3 Lima wood...............56 parts
Soda crystals......42 parts
Alum.............56 parts
Extract the color from the woods as for rose pink, and next boil the soda and alum together and add to the woods solution cold. This must be washed clean before adding to the wood liquor.
Water.............. 42 gallons
Cochineal........... 12 pounds
Salts of tartar....... 1.5 pounds
Potash alum........ J pound
Nitrous acid, nitromuriate of tin..... 44 pounds
Muriatic acid, nitromuriate of tin..... 60 pounds
Pure block tin, nitro-
muriate of tin..... 22 pounds
Should give specific gravity 1.310. Boil the water with close steam, taking care that no iron touches it; add the cochineal and boil for not more than five minutes; then turn off the steam and add salts of tartar and afterwards carefully add the alum. If it should not rise, put on steam until it does, pass through a 120-mesh sieve into a settling vat, and let it stand for 48 hours (not for precipitation). Add gradually nitromuriate of tin until the test on blotting paper (given below) shows that the separation is complete. Draw off clear water after it has settled, and filter. To test, rub a little of the paste on blotting paper, then dry on steam chest or on the hand, and if on bending it cracks, too much tin has been used.
Put a drop of color on white blotting paper, and if the color spreads, it is not precipitating. If there is a colorless ring around the spot of color it shows that precipitation is taking place; if the white ring is too strong, too much has been used.
 
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