This section is from the "Henley's Twentieth Century Formulas Recipes Processes" encyclopedia, by Norman W. Henley and others.
The article ought first to be cleaned with either nitric acid or muriatic acid, then immersed in an acid affecting the metal and dried in a warm place. A light coating is thus formed. For a second coating acetic or formic acid is used preferably for aluminum, nickel, and copper; but for iron and steel, muriatic or nitric acid. After cleaning, the article is placed in a solution of tannin or gallic acid, and is then dried in a warm place as before. The second coating is of a yellowish-brown color. On placing it near the fire, the color can be deepened until it becomes completely black; care must be taken to withdraw it when the desired shade is produced. Instead of the acids employed for the first coating, ammonia may be used.
 
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