* From the report of a committee of the American Society for Testing Materials.

For this purpose the Vicat Needle, which has already been described, should be used. In making the test, a paste of normal consistency is moulded and placed under the rod L, Fig. 2, as described in a previous paragraph. This rod bears the cap D at one end and the needle H, 1 mm. (0.039 in.) in diameter, at the other, and weighs 300 gr. (10.58 oz.). The needle is then carefully brought in contact with the surface of the paste and quickly released. The setting is said to have commenced when the needle ceases to pass a point 5 mm. (0.20 in.) above the upper surface of the glass plate, and is said to have terminated the moment the needle does not sink visibly into the mass.

The test pieces should be stored in moist air during the test; this is accomplished by placing them on a rack over water contained in a pan and covered with a damp cloth, the cloth to be kept away from them by means of a wire screen; or they may be stored in a moist box or closet. Care should be taken to keep the needle clean, as the collection of cement on the sides of the needle retards the penetration, while cement on the point reduces the area and tends to increase the penetration. The determination of the time of setting is only approximate, being materially affected by the temperature of the mixing water, the temperature and humidity of the air during the test, the percentage of water used, and the amount of moulding the paste receives.

The following approximate method, not requiring the use of apparatus, is sometimes used, although not referred to by the Committee. Spread cement paste of the proper consistency on a piece of glass, having the cement cake about three inches in diameter and about one inch thick at the center, thinning towards the edges. When the cake is hard enough to bear a gentle pressure of the finger nail, the cement has begun to set, and when it is not indented by a considerable pressure of the thumb nail, it is said to have set.

51. Standard Sand

The Committee recognizes the grave objections to the standard quartz now generally used, especially on account of its high percentage of voids, the difficulty of compacting in the moulds, and its lack of uniformity; it has spent much time in investigating the various natural sands which appeared to be available and suitable for use. For the present, the Committee recommends the natural sand from Ottawa, 111., screened to pass a sieve having 20 meshes per linear inch and retained on a sieve having 30 meshes per linear inch; the wires to have diameters of 0.0165 and 0.0112 inches, respectively, i.e., half the width of the opening in each case. Sand having passed the No. 20 sieve shall be considered standard when not more than one per cent passes a No. 30 sieve after one minute continuous sifting of a 500-gram sample.

52. Form Of Briquette

While the form of the briquette recommended by a former Committee of the Society is not wholly satisfactory, this Committee is not prepared to suggest any change, other than rounding off the corners by curves of 1/2-inch radius, Fig. 3.

Fig. 3. Form of Briquette.

Fig. 3. Form of Briquette.

53. Moulds

The moulds should be made of brass, bronze, or some equally non-corrodible material, having sufficient metal in the sides to prevent spreading during moulding.

Gang moulds, which permit moulding a number of briquettes at one time, are preferred by many to single moulds; since the greater quantity of mortar that can be mixed tends to produce greater uniformity in the results. The type shown in Fig. 4 is recommended. The moulds should be wiped with an oily cloth before using.

Fig. 4. Gang Moulds.

Fig. 4. Gang Moulds.

54. Mixing

All proportions should be stated by weight; the quantity of water to be used should be stated as a percentage of the dry material. The metric system is recommended because of the convenient relation of the gram and the cubic centimeter. The temperature of the room and the mixing water should be as near 21° Cent. (70° Fahr.) as it is practicable to maintain it. The sand and cement should be thoroughly mixed dry. The mixing should be done on some non-absorbing surface, preferably plate glass. If the mixing must be done on an absorbing surface it should be thoroughly dampened prior to use. The quantity of material to be mixed at one time depends on the number of test pieces to be made; about 1000 gr. (35.28 oz.) makes a convenient quantity to mix, especially by hand methods.

The material is weighed and placed on the mixing table, and a crater formed in the center, into which the proper percentage of clean water is poured; the material on the outer edge is turned into the crater by the aid of a trowel. As soon as the water has been absorbed, which should not require more than one minute, the operation is completed by vigorously kneading with the hands for an additional 1 1/2 minutes, the process being similar to that used in kneading dough. A sand-glass affords a convenient guide for the time of kneading. During the operation of mixing the hands should be protected by gloves, preferably of rubber.

55. Moulding

Having worked the paste or mortar to the proper consistency, it is at once placed in the moulds by hand. The moulds should be filled at once, the material pressed in firmly with the fingers and smoothed off with a trowel without ramming; the material should be heaped up on the upper surface of the mould, and, in smoothing off, the trowel should be drawn over the mould in such a manner as to exert a moderate pressure on the excess material. The mould should be turned over and the operation repeated. A check upon the uniformity of the mixing and moulding is afforded by weighing the briquettes just prior to immersion, or upon removal from the moist closet. Briquettes which vary in weight more than 3 per cent from the average should not be tested.